IS 1580:1991 ( Reaffirmed 2000 ) + f3y f~mlc\ - hzdian Standard BITUMINOUS COMPOUNDS FOR WATERPROOFING AND CAULKING PURPOSES - SPECIFICATION ( Second Revision ) First Reprint DECEMBER 1996 UDC 691'16 : 699'82 @ BIS 1991 BUREAU MANAK OF BHAVAN, INDIAN STANDARDS ZAFAR MARG 9 BAHADUR SHAH NEW DELHI 110002 July 1991 Prioc Group 2 Waterproofing and Damp-Proofing Sectional Committee, CED 41 FOREWORD This Indian Standard ( Second Revision ) was adopted by the Bureau of Indian Standards, after the draft finalized by the Waterproofing and Damp-Proofing Sectional Committee had been approved by the Civil Engineering Division Council. This standard was first published as specification for bitumen ( plastic ) for waterproofing purposes. In 1969 it was revised with a new title as specilication for bituminous compounds for waterproofing and caulking purposes. Since then other uses of the compound have also been experienced which necessitated the need of second revision of the standard. In this revision, besides incorporating three amendments earlier issued, two grades of bituminous material based on consistencies have been specified. Bituminous compound is suitable for cold application and has several uses. It may be used for stopping leaks and waterproofing porous masonry or as waterproofing compound to be applied on bolts head and overlapping joints in GI and asbestos sheets used for roofing. This also serves as caulking agent to be used for joints in drainpipe<, asbestos and CI pipes for crevices, vertical joints between steel plates and fold sections, wood joints, precast concrete cladding block, plate joints of railway wagon and buses. A compound of this type with some alteration is also used for fixing rainguard of polyethelene sheets on rubber trees. Since the materials conforming to this standard are required to meet widely different uses, the consisA material of thick consistel:cy required for filling wide cracks of roofs and tency has to be different. for capping bolt heads of GI and asbestos roof while of thin consistency for plate joints of wagons and buses and for fixing rainguards. For the purpose of deciding whether a particular requirement of this standard is complied with, the final value, observed or calculated, expressing the result of a test or analysis, shall be rounded off in accordance,with IS 2 : 1960 `Rules for rounding off numerical values ( revised )`. The number of significant places retained in the rounded off value should be the same as that of the specified value in this standard. IS 1580 : 1991 Indian Standard BITUMINOUS COMPOUNDS FOR WATERPROOFING AND CAULKING PURPOSES-SPECIFICATION ( Second 1 SCOPE Tevision ) 4 REQUIREMENTS 4.1 Grades Materials shall be of two grades : namely, Grade 1 and Grade 2 a) Grade I - shall be semistiff, smooth and homogenous paste suitable for application by spreading with hand, trowel, spatula or gun. b) Grade 2 - shall be of light consistency and homogenous paste suitable for application by putty knife. 4.2 Composition 4.2.1 The material shall consist of bitumen and flux oils with or without addition of vegetable or resinous oils, cut back with volatile thinners and intimately mixed with non-gritty absorbent, inorganic fibrous material ( with or without powder ) in suitable. proportions as to comply with the requirements of this standard. 4.2.2 The material shall also comply requirements specified in Table 1. 4.3 Keeping Quality When stored under cover in a dry place in the original sealed containerunder normal temperature the material shall retain the specified properties for a period of not less than six months from the date of manufacture as declared on container. 5 TESTS Test shall be carried out by the methods specified in co1 5 of Table 1. 6 SAMPLING The representative sample of the material be drawn as specified in IS 1201 : 1978. 7 PACKING The material shall be packed as agreed to between the manufacturer and the purchaser. 1 This standard specifies requirements and methods of sampling and tests for bituminous compounds, applied cold and used for stopping leaks through cracks of roofs, tioors, walls, etc; as sealant for plate joints of wagons, coaches and buses; as caulking agent for crevices and vertical joints between steel plates, folded sections, wood joints, precast concrete cladding, etc; and as adhesives for rainguards for rubber trees. 2 REFERENCES The Indian Standards listed below are necessary adjuncts to this standard: IS No. Title 334 : 1982 1201 : 1978 Glossary of terms relating to bitumen and tar (second revision) Methods for testing tar and bituminous materials; sampling (first revision ); 1209 : 1978 Methods for testing tar and bituminous materials; Determination of flash point and fire point (first revision ) with the 1211 : 1978 Methods for testing tar and bituminous materials; Determination of water content ( Dean and Stark method ) (first revision ) Methods for testing tar and bituminous materials; Determination of mineral matter ( ash ) (first Glossary of terms relating to bituminous waterproofing and damp-proofing of buildings (first revision ) 1217: 1978 revision ) 4911 : 1986 shall 3 TERMINOLOGY For the purpose of this standard definitions given in IS 334 : 1982 and IS 4911 : 1986 shall apply. IS 1580 :, 1991 8 MARKING 8.1 The containers shall following informations: be marked to give c) Grade of material, d) Date of manufacture. 8.2 The containers Standard Mark. may also be marked with the - a) Indication of the source of manufacture, b) Name of material, Table 1 Requirements for Bituminous Compounds ( Clauses 4.2.2 and 5 ) Sl No. Characteristic r_----& Requirements Grade 1 Grade 2 ' (4) 0'5 30 Shall satisfy the requirement 35 Shall satisfy' the requirement Method of Test' Ref to (5) IS 1211 : 1978 IS 1217 : 1978 Annex A IS 1209 : 1978 (1) i) ii) iii) iv) v) vi) (2) Water content, percent by mass, Max Ash content, percent by mass, Max Flow Flash point ,%, Min Flexibility and adhesion (3) 0'5 40 Shall satisfy requirement 35 Shall satisfy requirement the the Annex B Consistency a) Before setting ( test after 1 h ) Min 225 100 b) After setting ( test after 24 h ) Min 80 200 1 However. the temperature for test shall be stringent and kent at 10°C. Annex C ANNEX A [ Table 1, Item (iii) ] FLOW TEST A-l TEST SPECIMEN A-3 HEAT TEST Prepare a test film by applying the bitumen on 150 mm x 100 mm x 0'3 mm mild steel panel to a thickness of 3 mm. A-2 NORMAL TEST The film immediately after preparation as in A-l shall not show any slip when the panel is kept in a vertical position indoor at a temperature of 27 f 2°C for 5 h. The film shall not slip more than 6 mm when the panel is kept for 5 h in the vertical position in an air-dry oven maintained at 60 f 1°C. A-4 COLD TEST The film shall remain plastic and firmly adherent when the panel after treatment described in A-2 and A-3 is kept at OS-Jfor one hour. ANNEX FLEXIBILITY B-l TEST SPECIMEN B TEST [ TubZe 1, Item (v) ] AND ADHESION B-2 BEND TEST The film shall not The same test specimen that was used in the _ normal, heat and cold test, described in A-2, A-3. and A-4 shall be used for this test also. crack or flake off when the panel, after being subjected to the treatments described in A-2, A-3 and A-4 is bent double over a 25 mm diameter rod, with the film on the outside, at 27 f 2°C. 2 IS 1580: 1991 ANNEX C [ TubZe 1, Item (vi) ] CONSISTENCY C-l OUTLINE OF THE METHOD TEST CONE C-3 PENETRATION The penetration using a standard penetrometer is determined under specified temperature conditions by means of a standard cone applied to the specimen for 5 s under load of 150 g. C-2 PENETROMETER Any suitable penetrometer ( see Fig. I ) which The cone shall consist of a conical body of brass or corrosion resistant steel with detachable hardened steel tip, constructed to conform to the dimensions and tolerances shown in Fig. 2. The total moving mass, namely, that of the cone and its movable attachments shall be 150 + 0'1 g. The attachments consist of rigid shaft having a suitable device at its lower end for engaging the BE ROUNMO NO SHOULDER t"y All dimensions 0*3et*oe* 0.38: .a+ ALTERNATE MS!GN FOR EOGE in millimetrer. FIG. 1 PENETROMETER FIG. 2 PENETROMETER CONE permits the specified cone to drop vertically without appreciable friction for at least 40 mm and which indicates accurately the depth of penetration to the nearest 0'1 mm. The instrument shall have a table, to carry the test specimen which may be adjusted to the horizontal before making the test. A mechanism for releasing and clamping the loaded cone shall be provided. cone. The interior construction and dimensions may be modified to achieve the specified mass, provided the general contour and mass distribution are not altered. The outer surface should be polished to a very smooth finish. C-4 MASS OF TEST SPECIMEN At least 0'5 kg of the material shall be taken for test. 3 IS 1580 : 1991 C-5 PROCEDURE C-5.1 For Consistency 27f2"C for One Hour of the Sample Kept at penetrate the material for 5 s. Read the penetration on the penetrometer dial and express the consistency as penetration in tenths of mm. C-5.2 For Consistency 27312°C for 24 b of the Material Kept at Transfer the required quantity of the specimen to be tested into the penetration cup preferably in one lump and remove the entrapped air by gently tapping the sides of the cup. Fill the cup to the brim with specimen with least manipulation, without any air pockets. Immerse the cup with the specimen under water at 27f2"C and keep it for one hour. After one hour, place the cup on the penetrometer table, and adjust the cone assembly such that the tip of the cone just touches the surface of the material. The cone assembly should weigh 150+ 0'1 g, Release the cone assembly and alow it to The penetration of the test specimen and test procedure is exactly the same as given in C-5.1 except that the container filled with the specimen shall be kept under water at 27f2"C for 24 h. C-5.3 Additional Testing Average of three readings shall be taken on the same specimen if the consistency is less than 200, readings being observed at 120" apart. In case the consistency is more than 200, separate containers shall be filled with the materral and tested. 4 Hureau of Indian Standards BlS is a statutory institution established under the Brtwau ofhndian Stclndnrds Acl, 1986 to promote harmonious development of the activities of standardization, marking and quality certification of goods and attending to connected matters in the country. Copyright BIS has the copyright of all its publications. No part of these publications may be reproduced in any form without the prior permission in writing of BIS. This does not preclude the free use, in the course of implementing the standard, of necessary details, such as symbols and sizes, type or grade designations. Enquiries relating to copyright be addressed to the Director (Publications), BIS. Review of Indian Standards Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewed periodically; a standard along with amendments is reaffirmed when such review indicates that fro changes are needed; if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standards should ascertain that they are in possession of the latest amendments or edition by referring to the latest issue of `BIS Handbook' and `Standards Monthly Additions'. This Indian Standard has been developed from Dot : No. CED 41 ( 4537 1 Amendments Issued Since Publication Amend No. Date of Issue Text Affected BUREAU OF INDIAN STANDARDS Headquarters: Manak Bhavan, 9 Bahadur Shah Zafar Marg, New Delhi 110002 Telephones : 323 0131,323 c",3 75,323 94 02 Regional Offices : Central : Manak Bhavan, 9 Bahadur Shah Zafar Marg Telegrams : Manaksanstha (Common to all offices) Tclcphonc 323 76 17 1 323 38 41 337 84 99,337 8.5 61 { 337 86 20,337 9120 60 3x 43 { 60 20 2.5 235 02 16, 235 04 42 1 235 15 19,235 23 15 832 92 95,832 78 58 8327891,8327892 NEW DELHI 110002 Eastern : 1114 C. I.T. Scheme VII M, V. I. P. Road, Maniktola CALCUTTA 700054 Northern : SC0 335-336, Secto r 34-A, CHANDIGARH 100022 Southern : C. 1. T. Campus, IV Cross Road, MADRAS 600113 Western : Manakalaya, E9 MIDC, Marol, Andheri (East) MUMBAI 400093 Branches : AHMADABAD. BANGALORE. BHCPAL. BHUBANESHWAR. COIMBATORE. FARIDABAD. GHAZIABAD. GUWAHATI. HYDERABAD. JAIPUR. KAN-PUR. LUCKNOW. PATNA. 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